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Molecular mass determination via mass spectroscopy Mass spectra were obtained using LTQ Orbitrap Velos mass spectrometer (Thermo Fisher Scientific, Bremen, Germany) equipped with a nanospray ion source (electrospray voltage: 2.1 kV, ion transfer capillary temperature: 300 C), coupled to a nano HPLC-system (UltiMate 3000, Dionex)

doi: 10.1007/s11064-013-1199-5