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The peptide was cleaved from the 4.53 g peptide resin by treatment with 54 ml TFA/phenol/ethanedithiol/thioanisole/water 40:3:1:2:2 for 3 h at room temperature
PietinenPMalilaNVirtanenMHartmanTJTangreaJAAlbanesDet al
11 Mtodos de deteccin Mtodo de titulacin Procedimiento de anlisis: Pesar aproximadamente 0.1 g de la muestra secada hasta peso constante (precisin de 0.0001 g), aadir 20 mL de cido actico glacial y luego realizar una titulacin potenciomtrica con una solucin valorante estndar de cido perclrico (0.1 mol/L)
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Published 2012 Apr 18
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